HuagongsheHuagongshe Chemistry Print Report · For research reference only
Morpholine → HCID 22495934, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Morpholine | HCID 8083 | — |
| Reactant | HCID 22495894 | HCID 22495894 | — |
| Product | HCID 22495934 | HCID 22495934 | — |
Reaction Steps
20.00 g (0.56 mol) of 4-(5-chloro-2-nitro-benzoylamino)-benzenesulfonyl fluoride in 48.5 g (0.557 mol) of morpholine were heated under reflux for 1 h. Subsequently the mixture was cooled, poured onto ice/hydrochloric acid and filtered with suction. 26.0 g (98%) of the title compound having a melting point of 252° C. were obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07326789B2 |
| Source dataset | uspto-grants-2008_02 |
| ORD ID | ord-1da467bb8f0341c7a7775be2608f315e |
| Source note | uspto-grants-2008_02 |