Dichloroacetyl chloride → HCID 69224232, compound

HRID 2053389Notes

Reaction equation

HRID 2053389 reaction equation
[CH:1]([C:3]1[CH:9]=[CH:8][CH:7]=[CH:6][C:4]=1N)=[CH2:2].C([N:12](CC)CC)C.[Cl:17][CH:18]([Cl:22])[C:19](Cl)=[O:20]>ClCCl>[Cl:17][CH:18]([Cl:22])[C:19]([NH:12][C:6]1[CH:7]=[CH:8][CH:9]=[C:3]([CH:1]=[CH2:2])[CH:4]=1)=[O:20]

Participants

5

Reactant 3

HCID 6593Dichloroacetyl chlorideHCID 8471TriethylamineHCID 103516892-vinylaniline

Product 1

HCID 69224232HCID 69224232, compound

Reagents, catalysts & solvents 1

HCID 6344DichloromethaneSolvent

Procedure

Commercially available (Aldrich Chemical Co.) 2-vinylaniline can be dissolved in dichloromethane containing triethylamine and can be treated at 0° C. with dichloroacetyl chloride to yield 2.2-dichloro-N-(3-vinylphenyl)acetamide.

Sources & evidence

ORD record
ord-c8158ecd3acd4120a8d19ea51d4da061
Source dataset
uspto-grants-2008_02
Patent number
US07326790B2

Reaction notes

Loading…