HuagongsheHuagongshe Chemistry Print Report · For research reference only
3,3,3-Trifluoropropyne → HCID 22042604, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3,3,3-Trifluoropropyne | HCID 69578 | — |
| Reactant | HCID 22042580 | HCID 22042580 | — |
| Product | HCID 22042604 | HCID 22042604 | — |
Reaction Steps
The compound was prepared from N-methyl-N-(4-trifluoroacetyl-phenyl)-benzenesulfonamide (Example 22, Step A) and 3,3,3-trifluoroprop-1-yne following the procedure described in Example 29. 1H NMR (CDCl3) δ 3.19 (s, 3 H), 4.30 (br s, 1H), 7.11-7.63 (m, 9 H). Mass Spectrum (CI+) m/e=438 (M+1).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07326812B2 |
| Source dataset | uspto-grants-2008_02 |
| ORD ID | ord-fa4dc769a0724332a4909b74a8744ad1 |
| Source note | uspto-grants-2008_02 |