HuagongsheHuagongshe Chemistry Print Report · For research reference only
Diethyl Ether → HCID 69314856, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Diethyl Ether | HCID 3283 | — |
| Reactant | ethyl 2-oxo-2-(2-oxocyclopentyl)acetate | HCID 252487 | — |
| Reactant | HCID 69309751 | HCID 69309751 | — |
| Solvent | Acetic Acid | HCID 176 | — |
| Product | HCID 69314856 | HCID 69314856 | — |
Reaction Steps
4.0 g (18.2 mmol) of 4-hydrazino-3-trifluoromethylbenzoic acid is dissolved in 20 mL of glacial acetic acid, combined with 3.3 g (18.2 mmol) of ethyl oxo-(2-oxocyclopentyl)acetate, and refluxed for 2 hours under a nitrogen atmosphere. After cooling, it is stirred with diethyl ether and the precipitate is suction filtered. Yield: 2.9 g (43%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07326791B2 |
| Source dataset | uspto-grants-2008_02 |
| ORD ID | ord-9c8392d6b49440d094d5b51d738cbd7d |
| Source note | uspto-grants-2008_02 |