HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium Hydroxide → HCID 178464794, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium Hydroxide | HCID 14798 | — |
| Reactant | Chlorine | HCID 24526 | — |
| Reactant | HCID 178498064 | HCID 178498064 | — |
| Solvent | Isopropanol | HCID 3776 | — |
| Product | HCID 178464794 | HCID 178464794 | 85% |
Reaction Steps
Prepared analogously to Example 19b from rac.-3-chloro-N-[1-(5-chloro-1H-benzimidazol-2-yl)ethyl]-4-(2-methoxycarbonylpyrrolidin-1-ylcarbonyl)benzamide, and sodium hydroxide solution in isopropanol. Yield: 85%; C22H20Cl2N4O4 (475.33); mass spectrum: (M+H)+=475/477/479 (chlorine isotope).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07326791B2 |
| Source dataset | uspto-grants-2008_02 |
| ORD ID | ord-9d7fb4be814a4263bc3303956a79ef15 |
| Source note | uspto-grants-2008_02 |