N-Iodosuccinimide → HCID 11236615, compound

Participants

Reaction Steps

To a solution of 23a (10 mg, 0.03 mmol) in CH2Cl2 (5 ml) at −30° C. N-iodosuccinimide (7 mg mg, 0.03 mmol) was portionwise added and the mixture was stirred for 15 min. The solution was washed with water and the organic solutions was dried, filtered and evaporated to obtain 24a (14 mg, 95%) as a yellow solid.

Provenance & Evidence