HuagongsheHuagongshe Chemistry Print Report · For research reference only
Triethylamine → HCID 21938103, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Triethylamine | HCID 8471 | — |
| Reactant | Methyl Isocyanate | HCID 12228 | — |
| Reactant | HCID 21938176 | HCID 21938176 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 21938103 | HCID 21938103 | — |
Reaction Steps
100 mg of 4-[(1,2-diphenyl-1H-benzimidazol-6-yl)oxy]butan-1-ol was dissolved in 4 ml of dichloromethane, mixed with 0.1 ml of triethylamine and 20 mg of methyl isocyanate and stirred for 15 hours. Another 0.1 ml of triethylamine and 20 mg of methyl isocyanate were added, allowed to stir for 20 hours, and then concentrated by evaporation in a vacuum. The residue was purified using chromatography on silica gel.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07329679B2 |
| Source dataset | uspto-grants-2008_02 |
| ORD ID | ord-18f38ce8e50a46e1aeeeee3dbe46fe71 |
| Source note | uspto-grants-2008_02 |