Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | P-Anisidine | HCID 7732 | — |
| Reactant | 3-Fluoro-4-nitrophenol | HCID 520948 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 21937979 | HCID 21937979 | — |
Reaction Steps
0.16 g of 3-fluoro-4-nitrophenol and 0.37 g of p-anisidine were mixed and stirred for 1.5 hours at 150° C. After cooling, it was dissolved in dichloromethane, and extracted twice with 1N aqueous hydrochloric acid and once with saturated sodium chloride solution. The organic phase was dried on sodium sulfate and concentrated by evaporation in a vacuum.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US07329679B2 |
|---|
| Source dataset | uspto-grants-2008_02 |
|---|
| ORD ID | ord-6cb020c80e4d41c2ab9910463de69f0f |
|---|
| Source note | uspto-grants-2008_02 |
|---|
