Hydrochloric Acid → HCID 12282158, compound

HRID 2054639Notes

Reaction equation

HRID 2054639 reaction equation
[Cl:1][C:2]1[CH:9]=[CH:8][C:5]([C:6]#[N:7])=[CH:4][CH:3]=1.[CH2:10]([O:12]CC)[CH3:11].Cl>C(O)C>[ClH:1].[CH2:10]([O:12][C:6](=[NH:7])[C:5]1[CH:8]=[CH:9][C:2]([Cl:1])=[CH:3][CH:4]=1)[CH3:11]

Participants

5

Reactant 3

HCID 313Hydrochloric AcidHCID 3283Diethyl EtherHCID 121634-Chlorobenzonitrile

Product 1

HCID 12282158HCID 12282158, compound

Reagents, catalysts & solvents 1

HCID 702EthanolSolvent

Procedure

10 g of 4-chlorobenzonitrile was suspended in 12 ml of ethanol and dissolved by adding diethyl ether. While being cooled in an ice bath, it was saturated with HCl gas. After 72 hours, precipitated product was suctioned out. The product was washed with diethyl ether.

Workup

  1. dissolutiondissolved
  2. temperatureWhile being cooled in an ice bath
  3. customprecipitated product
  4. washThe product was washed with diethyl ether

Sources & evidence

ORD record
ord-231563f31ae040c99aa98ef43e98b912
Source dataset
uspto-grants-2008_02
Patent number
US07329679B2

Reaction notes

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