Sodium Chloride → HCID 11434990, compound

Participants

Reaction Steps

2E,4E-Hexadienoic acid 1 eq, ethyl chloroformate 1.12 eq, triethylamine 1.2 eq, ethylamine 1.5 eq as a 2.0M solution in THF, quench with 10% sodium chloride solution, yield=26%. 1.16 ppm (t, 3H, J=7.27 Hz), 1.82 ppm (d, 3H, J=6.09 Hz), 3.36 ppm (q, 2H, J=7.26 Hz, of d, J=5.73 Hz), 5.77 ppm (d, 1H, J=14.96 Hz), 5.93 ppm (br. s, 1H), 6.01-6.18 ppm (m, 2H), 7.19 ppm (d, 1H, J=14.94 Hz, oft, J=10.14 Hz).

Provenance & Evidence