HuagongsheHuagongshe Chemistry Print Report · For research reference only
5-Aminoquinoline → HCID 21948845, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 5-Aminoquinoline | HCID 11911 | — |
| Reactant | HCID 21948855 | HCID 21948855 | — |
| Solvent | Ethyl acetate hexane | HCID 21226206 | — |
| Product | HCID 21948845 | HCID 21948845 | 17.9% |
Reaction Steps
Analogously to Example 1, 300 mg (1.22 mmol) of 2-(2-methyl-2-phenylpropyl)-2-(trifluoromethyl)oxirane and 882 mg (6.12 mmol) of 5-aminoquinoline are reacted. After chromatography on silica gel with hexane-ethyl acetate (0-75%), 85 mg of product is obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07329753B2 |
| Source dataset | uspto-grants-2008_02 |
| ORD ID | ord-2ba6ec003b12487e991680302b028283 |
| Source note | uspto-grants-2008_02 |