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HRID2055056

反应详情

EQUATION

反应方程式

HRID 2055056 的结构方程式

REACTANTS

反应物

2
反应SMILES：CC(=O)n1c2ccccc2c2ccccc21
HCID95837

9H-Carbazole, 9-acetyl-

C14H11NO

反应SMILES：Clc1ccc2[nH]c3ccc(Cl)cc3c2c1
HCID236487

3,6-Dichlorocarbazole

C12H7Cl2N

PRODUCTS

产物

1
反应SMILES：CC(=O)Nc1cccc2c1[nH]c1ccccc12
HCID24832159

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

1
反应SMILES：CCO
溶剂HCID702

Ethanol

C2H6O

PROCEDURE

实验过程

Condensation of cyclohexane-1,4-dione 2 with phenylhydrazine 1 in ethanol affords the bishydrazone 3. Treatment of 3 with sulfuric acid and acetic acid produces 3-aminocarbazole 4 (Tetrahedron 2003, 59, 1265).