HuagongsheHuagongshe Chemistry Print Report · For research reference only
9-Acetyl-9H-carbazole → HCID 24832159, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 9-Acetyl-9H-carbazole | HCID 95837 | — |
| Reactant | 3,6-Dichlorocarbazole | HCID 236487 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 24832159 | HCID 24832159 | — |
Reaction Steps
Condensation of cyclohexane-1,4-dione 2 with phenylhydrazine 1 in ethanol affords the bishydrazone 3. Treatment of 3 with sulfuric acid and acetic acid produces 3-aminocarbazole 4 (Tetrahedron 2003, 59, 1265).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07331997B2 |
| Source dataset | uspto-grants-2008_02 |
| ORD ID | ord-fe0875d0591e4385a9caabaaa835377b |
| Source note | uspto-grants-2008_02 |