HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 69057349, compound → HCID 86606198, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 69057349 | HCID 69057349 | — |
| Catalyst | Iron | HCID 23925 | — |
| Product | HCID 86606198 | HCID 86606198 | 60% |
Reaction Steps
N1-benzyl-N4-(4-nitrophenacyl)piperazine dihydrochloride (IV-9) (2 mmol) was reduced by reductive iron in a procedure similar to Example 12 to give compound (IV-16), yield 60%, mp 286-288° C. M+ 309.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07332495B2 |
| Source dataset | uspto-grants-2008_02 |
| ORD ID | ord-c0bcef84032e48ae8e8a0a96b103cac0 |
| Source note | uspto-grants-2008_02 |