HuagongsheHuagongshe Chemistry Print Report · For research reference only
Potassium Carbonate → HCID 86606202, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | 3-Methoxybenzyl chloride | HCID 69994 | — |
| Reactant | 1-Phenyl-2-(piperazin-1-yl)ethan-1-one--hydrogen chloride (1/2) | HCID 23080512 | — |
| Solvent | Acetone | HCID 180 | — |
| Product | HCID 86606202 | HCID 86606202 | 54% |
Reaction Steps
A mixture of 3-methoxybenzylchloride (0.5 g, 2.15 mmol), N-phenacyl piperazine dihydrochloride (0.6 g, 2.15 mmol) and K2CO3 (1.04 g, 7.52 mmol) in 30 ml of acetone was treated according to general preparation 2 to give 0.46 g of compound (IV-25), yield 54%. M+ 324.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07332495B2 |
| Source dataset | uspto-grants-2008_02 |
| ORD ID | ord-4d5c529af5484fae8219fea7d5bee01d |
| Source note | uspto-grants-2008_02 |