Potassium Carbonate → HCID 131726773, compound

Participants

Reaction Steps

A mixture of N-(3,4-methylenedioxobenzyl)piperazine dihydrochloride (1 g, 4.5 mmol), 2-chloro-1-(5-chloro-6-methoxynaphthalen-2-yl)propan-1-one (1.54 g, 5.4 mmol) and K2CO3 (1.57 g, 11.25 mmol) in 20 ml of DMF, was treated according to general preparation 2 to give 0.62 g of compound (IV-30), yield 70%, mp 230-232° C. M+ 466.

Provenance & Evidence