HuagongsheHuagongshe Chemistry Print Report · For research reference only
Water → HCID 69202998, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Water | HCID 962 | — |
| Reactant | HCID 69202644 | HCID 69202644 | — |
| Catalyst | Iron | HCID 23925 | — |
| Solvent | Ammonium Chloride | HCID 25517 | — |
| Product | HCID 69202998 | HCID 69202998 | 172.3% |
Reaction Steps
A mixture of reductive iron (0.36 g, 6.47 mmol) in 8.5 ml of 5% NH4Cl, N1-(4-nitrobenzyl)-N4-[1-(5-chloro-6-methoxy-2-naphthoyl)ethyl]piperazine (IV-32) (0.5 g, 0.92 mmol) and water (10 ml) was stirred for 5 hours, and processed according to the procedure of example 12 to give 0.27 g of compound (IV-33), yield 60%, mp 206-8° C., M+ 437.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07332495B2 |
| Source dataset | uspto-grants-2008_02 |
| ORD ID | ord-690fd6d4c75d407a92902e5beb28e020 |
| Source note | uspto-grants-2008_02 |