HuagongsheHuagongshe Chemistry Print Report · For research reference only
tert-butyl N-(pyrrolidin-3-yl)carbamate → HCID 86596620, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | tert-butyl N-(pyrrolidin-3-yl)carbamate | HCID 2757234 | — |
| Reactant | 2-Chloro-5-iodopyridine | HCID 4397176 | — |
| Product | HCID 86596620 | HCID 86596620 | 48% |
Reaction Steps
tert-Butyl 3-pyrrolidinylcarbamate (0.377 g, 2.03 mmol; TCI) and 2-chloro-5-iodopyridine (0.484 g, 2.03 mmol; Aldrich) were processed according to the procedure of Example 1A to provide the title compound (0.29 g, 48%). MS (CI/NH3) m/z 298/300 (M+H)+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07332504B2 |
| Source dataset | uspto-grants-2008_02 |
| ORD ID | ord-72eff20ff4794e0eadc5d5b1e272b136 |
| Source note | uspto-grants-2008_02 |