HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-(N-Boc-amino)piperidine → HCID 53486065, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-(N-Boc-amino)piperidine | HCID 723833 | — |
| Reactant | 2-Chloro-5-iodopyridine | HCID 4397176 | — |
| Product | HCID 53486065 | HCID 53486065 | 43.2% |
Reaction Steps
tert-butyl 4-piperidinylcarbamate (0.30 g, 1.50 mmol; Astatech) and 2-chloro-5-iodopyridine (0.287 g, 1.50 mmol; Aldrich) were processed according to the procedure of Example 1A to provide the title compound as a yellow oil (0.202 g, 43%). (DCI/NH3) m/z 312 (M+H)+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07332504B2 |
| Source dataset | uspto-grants-2008_02 |
| ORD ID | ord-2ccf345ead134ff0858b27aec36f0439 |
| Source note | uspto-grants-2008_02 |