HuagongsheHuagongshe Chemistry Print Report · For research reference only
Formamide → HCID 135553012, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Formamide | HCID 713 | — |
| Reactant | 2-Amino-3-bromo-5-chlorobenzoic acid | HCID 11779931 | — |
| Product | HCID 135553012 | HCID 135553012 | — |
Reaction Steps
8-Bromo-6-chloro-4(3H) quinazolinone was prepared from 2-amino-3-bromo-5-chlorobenzoic acid (10 g, 40 mmol). The acid was heated in excess formamide (50 mL) at reflux overnight. The mixture was cooled and quenched with water. The solid that formed was washed with acetonitrile, 6.7 g crude (65%); MS: 260.8 (M+H)+
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07332506B2 |
| Source dataset | uspto-grants-2008_02 |
| ORD ID | ord-4dd82de2a8234fc5b58672625743b906 |
| Source note | uspto-grants-2008_02 |