Methylamine → HCID 131726778, compound

HRID 2055691Notes

Reaction equation

HRID 2055691 reaction equation
[Cl:1][CH2:2][C:3]1[CH:8]=[CH:7][C:6]([C:9]2[O:13][N:12]=[C:11]([CH2:14][CH:15]3[CH2:20][CH2:19][N:18]([CH:21]4[CH2:25][CH2:24][CH2:23][CH2:22]4)[CH2:17][CH2:16]3)[N:10]=2)=[CH:5][CH:4]=1.[CH3:26][NH2:27]>>[ClH:1].[ClH:1].[CH:21]1([N:18]2[CH2:19][CH2:20][CH:15]([CH2:14][C:11]3[N:10]=[C:9]([C:6]4[CH:5]=[CH:4][C:3]([CH2:2][CH2:26][NH2:27])=[CH:8][CH:7]=4)[O:13][N:12]=3)[CH2:16][CH2:17]2)[CH2:22][CH2:23][CH2:24][CH2:25]1

Participants

3

Reactant 2

HCID 6329MethylamineHCID 68432098HCID 68432098, compound

Product 1

HCID 131726778HCID 131726778, compound

Procedure

The title compound was prepared by a similar procedure to that described in Example 23, starting from 4-[5-(4-chloromethylphenyl)[1,2,4]oxadiazol-3-ylmethyl]-1-cyclopentylpiperidine and methylamine. HPLC: Rt=4.89 min.

Sources & evidence

ORD record
ord-f99e3c78ebda4a279337325e2a65cbe8
Source dataset
uspto-grants-2008_02
Patent number
US07332508B2

Reaction notes

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