Chloride → N-[(Trimethoxysilyl)methyl]benzenamine

HRID 2055765Notes

Reaction equation

HRID 2055765 reaction equation
[CH3:1][O:2][Si:3]([CH2:8][N:9]([C:18]1[CH:23]=[CH:22][CH:21]=[CH:20][CH:19]=1)C[Si](OC)(OC)OC)([O:6][CH3:7])[O:4][CH3:5].[Cl-]>>[C:18]1([NH:9][CH2:8][Si:3]([O:6][CH3:7])([O:2][CH3:1])[O:4][CH3:5])[CH:19]=[CH:20][CH:21]=[CH:22][CH:23]=1

Participants

3

Reactant 2

HCID 312ChlorideHCID 21987730HCID 21987730, compound

Product 1

HCID 13975829N-[(Trimethoxysilyl)methyl]benzenamine

Procedure

A yield of 331.2 g, i.e., 75.9% of theory, is obtained, with a product purity of about 96.5%. The product contains about 3.5% of N,N-bis[trimethoxysilylmethyl]-phenylamine as an impurity. The resulting product possesses a chloride content of approximately 100 ppm.

Workup

  1. customA yield of 331.2 g, i.e., 75.9% of theory, is obtained, with a product purity of about 96.5%

Sources & evidence

ORD record
ord-ceb949c70c244bb9a79b376e8e43cc01
Source dataset
uspto-grants-2008_02
Patent number
US07332541B2

Reaction notes

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