1,2-Diiodobenzene → Silane, [(2-iodophenyl)ethynyl]trimethyl-

HRID 2055833Notes

Reaction equation

I[C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][C:3]=1[I:8].[CH3:9][Si:10]([C:13]#[CH:14])([CH3:12])[CH3:11]>>[CH3:9][Si:10]([CH3:12])([CH3:11])[C:13]#[C:14][C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][C:3]=1[I:8]

Participants

Reactant 2

HCID 119941,2-Diiodobenzene

HCID 66111Trimethylsilylacetylene

Product 1

HCID 10979486Silane, [(2-iodophenyl)ethynyl]trimethyl-Yield 54%

Procedure

The title compound was synthesized as a yellow oil in 54% yield using 1,2-diiodobenzene and (trimethylsilyl)acetylene as the starting materials according to Method A of the above-described General Synthesis Procedures I.

Workup

customaccording to Method A of the above-described General Synthesis Procedures I

Sources & evidence

ORD record: ord-4c371212c94741ab9fd0dd4a7a6a6c49
Source dataset: uspto-grants-2008_02
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US07332623B2

Reaction notes

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