HuagongsheHuagongshe Chemistry Print Report · For research reference only
Trimethylsilylacetylene → HCID 72741377, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Trimethylsilylacetylene | HCID 66111 | — |
| Reactant | HCID 11062498 | HCID 11062498 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Product | HCID 72741377 | HCID 72741377 | 53% |
Reaction Steps
According to Method A of the above-described General Synthesis Procedures I, the coupling reaction of compound (a4) from Example 4 with trimethylsilylacetylene using palladium as a catalyst gave the title compound (a5) as an oil in 53% yield.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07332623B2 |
| Source dataset | uspto-grants-2008_02 |
| ORD ID | ord-ef28960aa8f44053b2bcad6e6cdc3b22 |
| Source note | uspto-grants-2008_02 |