Bis(2-pyridylmethyl)amine → HCID 11515602, compound

Participants

Reaction Steps

In a 250 ml three-necked flask 1 equivalent of bis(2-pyridylmethyl)amine was dissolved in 100 ml of THF and the solution was admixed with 1 equivalent of 2,6-bis(chloromethyl)pyridine and 4 equivalents of N,N-diisopropylethylamide. The solution was stirred at room temperature for 7 days. The solution was filtered and the filtrate was purified by column chromatography.

Provenance & Evidence