huagongshe.com
HRID2057304

反应详情

EQUATION

反应方程式

HRID 2057304 的结构方程式

REACTANTS

反应物

4
结构：CNC
HCID674

Dimethylamine

C2H7N

结构：O=C(O)C(F)(F)F
HCID6422

未命名化合物

结构：O=S(=O)(Cl)c1ccc(C(F)(F)F)cc1
HCID2777399

4-(Trifluoromethyl)benzenesulfonyl chloride

C7H4ClF3O2S

结构：CN[C@H]1CC[C@H](CCCCOS(C)(=O)=O)CC1
HCID178484800

未命名化合物

PRODUCTS

生成物

1
结构：CN(C)CCCC[C@H]1CC[C@H](N(C)S(=O)(=O)c2ccc(C(F)(F)F)cc2)CC1
HCID178483442

未命名化合物

PROCEDURE

实验过程

In analogy to examples 31.5 and 31.6, trans-Methanesulfonic acid 4-(4-methylamino-cyclohexyl)-butyl ester.trifluoro-acetic acid and 4-trifluoromethyl-phenyl-sulfonylchloride were reacted, followed by treatment with dimethlamine to give trans-N-[4-(4-Dimethylamino-butyl)-cyclohexyl]-N-methyl-4-trifluoromethyl-benzenesulfonamide, MS: 421 (MH+).