HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 20231523, compound → HCID 20286840, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 20231523 | HCID 20231523 | — |
| Reactant | HCID 20332297 | HCID 20332297 | — |
| Product | HCID 20286840 | HCID 20286840 | — |
Reaction Steps
The procedure described in (a) is repeated, starting from 65 g (0.168 mole) of 3,12-dicyclooctyl-1,2-diazacyclododecane and using correspondingly reduced amounts of catalyst and solvent, affording after purification by chromatography 43.6 g (66% of theory) of 1,10-diamino-1,10-dicyclooctyldecane as a colourless oil [nD20 =1.5050; IR spectrum (liquid) includes bands at 3333, 3278, 1613 cm-1 ].
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04210742 |
| Source dataset | uspto-grants-1980_07 |
| ORD ID | ord-a6f42d2f314b4e6b85e3f154b2662737 |
| Source note | uspto-grants-1980_07 |