HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 20331375, compound → HCID 20331378, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 20331375 | HCID 20331375 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 20331378 | HCID 20331378 | — |
Reaction Steps
The product from step (b) (12 gm) was dissolved in ethanol (150 ml) and reduced with 5% palladium on carbon (1.2 gm) under an atmosphere of hydrogen (45 psi). The catalyst was removed by filtration and the ethanol was removed in vacuo to yield the product as a brown mobile oil. Wt 11.5 gm.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04211788 |
| Source dataset | uspto-grants-1980_07 |
| ORD ID | ord-2c85362625e944acbb065d8a61b74807 |
| Source note | uspto-grants-1980_07 |