HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ammonia → HCID 20331562, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ammonia | HCID 222 | — |
| Reactant | HCID 14714141 | HCID 14714141 | — |
| Solvent | Diethyl Ether | HCID 3283 | — |
| Product | HCID 20331562 | HCID 20331562 | — |
Reaction Steps
To 16.52 g (0.074 mole) of 9-fluorenylisothiocyanate in ether is added excess anhydrous NH3 with cooling. The reaction mixture is capped and allowed to stand overnight at 0° C. Filtration gives the product, N-(9-fluorenyl)-thiourea, m.p. (158°) 182°-189° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04211867 |
| Source dataset | uspto-grants-1980_07 |
| ORD ID | ord-bb34f21c353749e0bd68c1513e3fe4b9 |
| Source note | uspto-grants-1980_07 |