HuagongsheHuagongshe Chemistry Print Report · For research reference only
Diethyl Ether → HCID 178503962, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Diethyl Ether | HCID 3283 | — |
| Reactant | Methyl iodide | HCID 6328 | — |
| Reactant | HCID 20331562 | HCID 20331562 | — |
| Solvent | Acetone | HCID 180 | — |
| Product | HCID 178503962 | HCID 178503962 | — |
Reaction Steps
To 7.85 g. (0.033 mole) of N-(9-fluorenyl)thiourea in 200 ml acetone is added 4.68 g (0.033 mole) of methyl iodide. The mixture is allowed to stand at room temperature for about 4 hours. Ether (400 ml) is added and the mixture allowed to stand overnight, affording the crystalline product, methyl N-(9-fluorenyl)carbamimidothioate hydroiodide, which is filtered off; m.p. (208) 212°-14° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04211867 |
| Source dataset | uspto-grants-1980_07 |
| ORD ID | ord-8d4f22b6387b46ebaa285bfdb5a68d6c |
| Source note | uspto-grants-1980_07 |