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HRID2057646

反应详情

EQUATION

反应方程式

HRID 2057646 的结构方程式

REACTANTS

反应物

4
结构：Cc1ccccc1
HCID1140

Toluene

C7H8

结构：O=[N+]([O-])c1ccc(S(=O)(=O)O)c([N+](=O)[O-])c1
HCID6959

2,4-Dinitrobenzenesulfonic acid

C6H4N2O7S

结构：CCOC(=O)CCc1ccc(N)cc1
HCID10442595

Ethyl 3-(4-aminophenyl)propanoate

C11H15NO2

结构：CCCCCCCCc1ccc(C=O)s1
HCID13791588

5-Octylthiophene-2-carbaldehyde

C13H20OS

PRODUCTS

生成物

1
结构：CCCCCCCCC1=CCC(=Nc2ccc(CCC(=O)OCC)cc2)S1
HCID20331197

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

1
结构：O
溶剂HCID962

Water

H2O

PROCEDURE

实验过程

A solution of 8.6 g. ethyl 4-aminohydrocinnamate, 9.77 g. 5-octyl-2-thiophenecarboxaldehyde and a few crystals of 2,4-dinitrobenzenesulfonic acid in 250 ml. toluene is refluxed under a Dean-Stark trap for 17 hours, whereupon the theoretical amount (0.8 ml.) water has been collected. The toluene is evaporated to yield ethyl 3-[4-(5-octyl-2-thienylideneamino)phenyl]propionate as a crystalline mass.

WORKUP

后处理

  1. customhas been collected
  2. customThe toluene is evaporated