HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Pyridinecarboxaldehyde → HCID 78605778, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Pyridinecarboxaldehyde | HCID 14273 | — |
| Reactant | Hydrazine, (4-chlorophenyl)-, hydrochloride (1:1) | HCID 71600 | — |
| Reactant | Sodium Acetate | HCID 517045 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 78605778 | HCID 78605778 | — |
Reaction Steps
2.2 g of 2-pyridinecarbaldehyde was added to a mixture of 3.6 g of p-chlorophenylhydrazine hydrochloride and 9.8 g of sodium acetate in 60 ml of 50% by volume aqueous ethyl alcohol. The mixture was refluxed for 10 minutes, cooled and the precipitate crystallized from ethyl alcohol to give 2, as yellow crystals, mp 184°-186° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04212868 |
| Source dataset | uspto-grants-1980_07 |
| ORD ID | ord-f03605f405c94c128ebbb79d84968ac5 |
| Source note | uspto-grants-1980_07 |