HuagongsheHuagongshe Chemistry Print Report · For research reference only
Isopropanol → HCID 20330162, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Isopropanol | HCID 3776 | — |
| Reactant | Acetic Anhydride | HCID 7918 | — |
| Reactant | HCID 20330193 | HCID 20330193 | — |
| Solvent | Water | HCID 962 | — |
| Product | HCID 20330162 | HCID 20330162 | — |
Reaction Steps
To a 0.33 g. sample of 5-amino-2-nitro-3-phenylbenzofuran is added 1 ml. of acetic anhydride, and the mixture is heated for 5 minutes on a steam bath. About 10 ml. of isopropanol is added, and the mixture is again heated on a steam bath to dissolve the solid. It is then saturated with hot water and cooled to provide yellow needles of 5-acetamido-2-nitro-3-phenylbenzofuran, m.p. 204°-207° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04212865 |
| Source dataset | uspto-grants-1980_07 |
| ORD ID | ord-52031e06250340e29a3aaf85c354b506 |
| Source note | uspto-grants-1980_07 |