HuagongsheHuagongshe Chemistry Print Report · For research reference only
m-Nitroacetophenone → 2-Bromo-1-(3-nitrophenyl)ethan-1-one
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | m-Nitroacetophenone | HCID 8494 | — |
| Reactant | Bromine | HCID 24408 | — |
| Solvent | Chloroform | HCID 6212 | — |
| Product | 2-Bromo-1-(3-nitrophenyl)ethan-1-one | HCID 75213 | — |
Reaction Steps
60 g. of 3-nitroacetophenone in 250 ml. of chloroform is treated with 58.2 g. of bromine in 50 ml. of chloroform. The solvent is evaporated and the product separated by filtration and recrystallized from benzene to provide α-bromo-3-nitroacetophenone, m.p. 91°-94° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04212865 |
| Source dataset | uspto-grants-1980_07 |
| ORD ID | ord-fd438164c85843e8bbe14faa0046be0f |
| Source note | uspto-grants-1980_07 |