HRID2057862

反应详情

EQUATION

反应方程式

HRID 2057862 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

2

PROCEDURE

实验过程

A solution prepared by dissolving 11 g of capric acid in 100 ml of butyl acetate was mixed with a solution prepared by dissolving 1.8 g of sodium hydroxide in 150 ml of water and, further, 0.25 g of ammonium bromide and 0.02 g of ammonium iodide were added thereto, followed by stirring with a homogenizer at 1500 rpm to emulsify the system. While stirring, an aqueous solution prepared by dissolving 8.5 g of silver nitrate in 50 ml of water was added thereto to yield both silver halide and silver caprate. This reaction system separated into two phases when allowed to stand. An aqueous phase, one of the two phases, was removed, and the remaining butyl acetate phase containing silver caprate and silver halide (silver caprate: ca. 1/20 mol, AgX: ca. 2.5×10-3 mol) was dispersed in a 15 wt% isopropanol solution of polyvinyl butyral to prepare a polymer dispersion of the silver salts. This solution was referred to as dispersion K.

WORKUP

后处理

  1. customA solution prepared
  2. additionwas mixed with a solution
  3. customprepared
  4. stirringWhile stirring
  5. customan aqueous solution prepared
  6. additionwas added