HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 86737097, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | Ethanethiol | HCID 6343 | — |
| Reactant | 1-Methyl-5-(p-toluoyl)pyrrole-2-acetonitrile | HCID 11107405 | — |
| Reactant | Sodium 1-methyl-5-(p-toluoyl)-pyrrole-2-acetic acid | HCID 66584587 | — |
| Product | HCID 86737097 | HCID 86737097 | — |
Reaction Steps
A process of preparing sodium 1-methyl-5-(p-toluoyl)- pyrrole-2-acetic acid which comprises reacting 1-methyl-5- (p-toluoyl)pyrrole-2-acetonitrile with ethyl mercaptan in the presence of hydrogen chloride in an anhydrous aprotic organic solvent under an inert atmosphere at or below 10° C. to yield ethyl 1-methyl-5-(p-toluoyl)pyrrole-2-thiolacetate and then hydrolyzing said thiolacetate by treatment with aqueous sodium hydroxide.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04213905 |
| Source dataset | uspto-grants-1980_07 |
| ORD ID | ord-46cfd9a08d82413495c18df103be3179 |
| Source note | uspto-grants-1980_07 |