HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Chloropropionyl chloride → HCID 20256761, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Chloropropionyl chloride | HCID 111019 | — |
| Reactant | HCID 12184078 | HCID 12184078 | — |
| Solvent | 1,4-Dioxane | HCID 31275 | — |
| Product | HCID 20256761 | HCID 20256761 | — |
Reaction Steps
A solution of 2-chloropropionyl chloride and 5-methyl-5,11-dihydro-6H-pyrido-[2,3-b][1,4]-benzodiazepine-6-one in dioxane was reacted to obtain 11-(2-chloropropionyl)-5,11-dihydro-6H-pyrido-[2,3-b][1,4]-benzodiazepine-6-one which after crystallization from acetonitrile melted at 210°-212° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04213985 |
| Source dataset | uspto-grants-1980_07 |
| ORD ID | ord-e61895ef6c2a4c94a4ffb6d90c8ad757 |
| Source note | uspto-grants-1980_07 |