HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-(2-Methylallyl)piperazine → HCID 20329389, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-(2-Methylallyl)piperazine | HCID 1073878 | — |
| Reactant | 11-(3-chloropropionyl)-5,11-dihydro-6H-pyrido[2,3-b][1,4]benzodiazepin-6-one | HCID 13810571 | — |
| Product | HCID 20329389 | HCID 20329389 | 45% |
Reaction Steps
Using the procedure of Example 2, 11-(3-chloropropionyl)-5,11-dihydro-6H-pyrido-[2,3-b][1,4]-benzodiazepine-6-one was reacted with 1-(2-methyl-allyl)-piperazine to obtain a 45% yield of 5,11-dihydro-11-{3-[4-(2-methyl-allyl)-1-piperazinyl]-propionyl}-6H-pyrido-[2,3-b][1,4]-benzodiazepine-6-one melting at 210°-211° C. after crystallization from ethanol.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04213985 |
| Source dataset | uspto-grants-1980_07 |
| ORD ID | ord-fbefbd71dd8e429b8f6c1b764342a555 |
| Source note | uspto-grants-1980_07 |