HuagongsheHuagongshe Chemistry Print Report · For research reference only
Nitric Acid → HCID 70506468, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Nitric Acid | HCID 944 | — |
| Reactant | HCID 20329506 | HCID 20329506 | — |
| Solvent | Diethyl Ether | HCID 3283 | — |
| Product | HCID 70506468 | HCID 70506468 | — |
Reaction Steps
Nitric acid (70%; d=1.42) was added dropwise to a stirred solution of 2.0 g of 1-[2-(2-chlorophenylthio)-4-(4-methoxyphenyl)-n-butyl]imidazole in 30 ml of anhydrous ether until precipitation was complete. The product was filtered off, washed with ether, air dried, and recrystallized from ethyl acetate to yield 1-[2-(2-chlorophenylthio)-4-(4-methoxyphenyl)n-butyl]imidazole nitrate, mp 131.5°-133.5° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04213991 |
| Source dataset | uspto-grants-1980_07 |
| ORD ID | ord-f338cb54a3704ff4bede40784995ebd8 |
| Source note | uspto-grants-1980_07 |