Tert-Butylamine → HCID 20296727, compound

HRID 2057965Notes

Reaction equation

HRID 2057965 reaction equation
O([C:8]([NH:10][C:11]1[CH:16]=[CH:15][C:14]([C:17](=[O:20])[CH2:18][Br:19])=[CH:13][C:12]=1[C:21]#[N:22])=[O:9])C1C=CC=CC=1.[C:23]([NH2:27])([CH3:26])([CH3:25])[CH3:24]>>[C:23]([NH:27][C:8](=[O:9])[NH:10][C:11]1[CH:16]=[CH:15][C:14]([C:17](=[O:20])[CH2:18][Br:19])=[CH:13][C:12]=1[C:21]#[N:22])([CH3:26])([CH3:25])[CH3:24]

Participants

3

Reactant 2

HCID 6385Tert-ButylamineHCID 20296729HCID 20296729, compound

Product 1

HCID 20296727HCID 20296727, compound

Procedure

The starting compound, 4'-(3-tert. butyl-ureido)-2-bromo-3'-cyano-acetophenone was prepared by reacting 4'-phenoxycarbonylamino-2-bromo-3'-cyanoacetophenone with tert. butylamine at room temperature.

Workup

  1. customat room temperature

Sources & evidence

ORD record
ord-c6546531cba64a86add8fbdebbc0dbd0
Source dataset
uspto-grants-1980_07
Patent number
US04214001

Reaction notes

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