HCID 20329754, compound → HCID 20329796, compound

Participants

Reaction Steps

A 1.0-g portion of the phenyl 7-nitro-1,2,3,4-tetrahydro-1-naphthoate obtained above was catalytically reduced with 5% palladium-carbon in ethyl acetate. After removal of the catalyst by filtration, the ethyl acetate was removed by distillation under reduced pressure. The residue was recrystallized from methanol to obtain 550 mg of phenyl 7-amino-1,2,3,4-tetrahydro-1-naphthoate, m.p. 89°-90° C.

Provenance & Evidence