HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methyl Isocyanate → HCID 54329214, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methyl Isocyanate | HCID 12228 | — |
| Reactant | HCID 86737114 | HCID 86737114 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 54329214 | HCID 54329214 | — |
Reaction Steps
To 50 mg of 3,3-dimethyl-1-(methylsulfinyl)-1-methylthio-2-butanone oxime in 5 ml of methylene chloride is added 0.5 ml of methyl isocyanate. After standing at room temperature 18 hrs., the solvent was removed to give 53 mg of impure 3,3-dimethyl-1-(methylsulfinyl)-1-methylthio-2-butanone O-[methylaminocarbonyl]oxime. The ir and pmr were identical to that of an authentic sample synthesized independently.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04215075 |
| Source dataset | uspto-grants-1980_07 |
| ORD ID | ord-7b099a16137e40698c1355050db92162 |
| Source note | uspto-grants-1980_07 |