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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 2058440Generated: November 1, 2026

HCID 12837422, compound → HCID 86738275, compound

https://huagongshe.com/reaction/2058440

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHCID 12837422HCID 12837422—
ReactantHCID 178418287HCID 178418287—
ProductHCID 86738275HCID 86738275—

Reaction Steps

4-Diazo-17β-hydroxymethyl-5αandrostan-3-one is oxidized with pyridinium chlorochromate according to the procedure described in Example 4 to give 4-diazo-3-oxo-5α-androstane-17β-carboxaldehyde. In a similar manner, 4-diazo-17β-hydroxy-5α-androstan-3-one is oxidized with pyridinium chlorochromate to give 4-diazo-5α-androstane-3,17-dione.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS04317817
Source datasetuspto-grants-1982_03
ORD IDord-8074ad248aa44f82a7b894e592e281fa
Source noteuspto-grants-1982_03