HRID2058442

反应详情

EQUATION

反应方程式

HRID 2058442 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

1

PROCEDURE

实验过程

Imidazole (2.0 g, 0.03 mol) was added to a solution of sodium (0.7 g, 0.03 mol) in dry ethanol (50 ml). The mixture was stirred and heated to boiling when bromomethylcyclooctane (5.5 g, 0.027 mol) was added dropwise. Following the addition, the reaction mixture was stirred and boiled for 15 h.

WORKUP

后处理

  1. temperatureheated
  2. additionwas added dropwise
  3. additionthe addition
  4. stirringthe reaction mixture was stirred