HuagongsheHuagongshe Chemistry Print Report · For research reference only
Imidazole → HCID 20550244, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Imidazole | HCID 795 | — |
| Reactant | 1-(Bromomethyl)-4-methylcyclohexane | HCID 13460364 | — |
| Reactant | Potassium tert-butoxide | HCID 23665647 | — |
| Solvent | 1-Butanol | HCID 263 | — |
| Product | HCID 20550244 | HCID 20550244 | — |
Reaction Steps
1-Bromomethyl-4-methylcyclohexane (3.1 g, 0.0162 mol) was added dropwise to a stirred, boiling solution of imidazole (1.12 g, 0.0165 mol) and potassium t-butoxide (1.85 g, 0.0165 mol) in dry n-butanol, under dry nitrogen. After the addition, the reaction mixture was stirred and heated under reflux for 10 h.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04317830 |
| Source dataset | uspto-grants-1982_03 |
| ORD ID | ord-bfaef8f7ff4b434dbd9c733d1c1916f0 |
| Source note | uspto-grants-1982_03 |