Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Succinic Acid → 1-Cyclooctylmethylimidazole hydrogen succinate
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Succinic Acid | HCID 1110 | — |
| 반응물 | 1-Cyclooctylmethylimidazole | HCID 20550238 | — |
| 용매 | Ethanol | HCID 702 | — |
| 생성물 | 1-Cyclooctylmethylimidazole hydrogen succinate | HCID 20550250 | 44.7% |
반응 단계
A solution of succinic acid (0.23 g) in ethanol (~5 ml) was added to a solution of 1-cyclooctylmethylimidazole (0.38 g) in ethanol (5 ml). Evaporation of the solution afforded a white solid. Recrystallisation of the solid from ethyl acetate afforded 1-cyclooctylmethylimidazole hydrogen succinate (0.27 g) as colourless plates, m.p. 86° to 87° C.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04317830 |
| 출처 데이터셋 | uspto-grants-1982_03 |
| ORD ID | ord-f3c8a4fd58044f61b41eedb23a9e3b99 |
| 출처 메모 | uspto-grants-1982_03 |