Hydrochloric Acid → HCID 85794228, compound

HRID 2058614Notes

Reaction equation

HRID 2058614 reaction equation
O(Cl)Cl.[Zr:4].Cl.[Si:6]([O-:10])([O-:9])([O-:8])[O-:7].[Na+].[Na+].[Na+].[Na+].[P:15](=[O:19])([OH:18])([OH:17])[OH:16]>O>[Si:6]([O-:10])([O-:9])([O-:8])[O-:7].[P:15]([OH:19])([OH:18])([OH:17])=[O:16].[Zr+4:4]

Participants

6

Reactant 4

HCID 313Hydrochloric AcidHCID 1004Phosphoric AcidHCID 26051Sodium orthosilicateHCID 71304769Chloro hypochlorite;zirconium

Product 1

HCID 85794228HCID 85794228, compound

Reagents, catalysts & solvents 1

HCID 962WaterSolvent3×

Procedure

Three hundred and twenty-two (322) g of zirconium oxychloride is dissolved in 3 liter of water, and to this solution is added 200 g of concentrated hydrochloric acid. To the resulting acidic solution are added the aqueous solution prepared by dissolving 552 g of sodium silicate (Na2SiO3) in 10 liter of water as well as the aqueous solution consisting of 100 g of 98% phosphoric acid and 3 liter of water, and, after stirred for about 30 minutes, precipitates of zirconium phosphate silicate formed in the solution are separated. The subsequent procedures are conducted in the same manner as in the above (1) to prepare particles of the desired compound.

Workup

  1. additionTo the resulting acidic solution are added the aqueous solution
  2. customprepared
  3. customprecipitates of zirconium phosphate silicate
  4. customformed in the solution
  5. customare separated
  6. customto prepare particles of the desired compound

Sources & evidence

ORD record
ord-2b7f4e9314d542a4904748cd6659d838
Source dataset
uspto-grants-1982_03
Patent number
US04318417

Reaction notes

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