HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 54467735, compound → HCID 20549077, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 54467735 | HCID 54467735 | — |
| Catalyst | Nickel | HCID 935 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 20549077 | HCID 20549077 | 94% |
Reaction Steps
A solution of 100 g (0.42 mole) of 2a in 300 mL of methanol was hydrogenated under standard conditions with 5 g of Raney nickel (ca. 10 hours). Filtration, distillation of the solvent, and fractionation yielded 94 g (94%) of 3a, b0.7 92°-95° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04318831 |
| Source dataset | uspto-grants-1982_03 |
| ORD ID | ord-d02534f1469249f0a777ab970e3ba541 |
| Source note | uspto-grants-1982_03 |