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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 2058651Generated: November 2, 2026

2-Methyl-2-thiopseudourea → HCID 140335238, compound

https://huagongshe.com/reaction/2058651

Reaction equation

Participants

RoleNameHCIDCharge
Reactant2-Methyl-2-thiopseudoureaHCID 5142—
ReactantHCID 20549424HCID 20549424—
SolventAcetoneHCID 180—
ProductHCID 140335238HCID 140335238—

Reaction Conditions

Temperature10 °C

Reaction Steps

To 7 g S-methylisothiourea in 50 ml of acetone at 10 degrees C., there are added in drops 12 g of 2-(2,6-dichlorophenyl)-2-bromo-acetyl bromide in 30 ml acetone. The mixture is stirred for 30 minutes at 10 degrees C., and the precipitate is suction-filtered. After concentration of the mother liquor, a second fraction of S-methyl-N-[2-(2,6-dichlorophenyl)-2-bromo acetyl] isothiourea is obtained. The decomposition point is 177 degrees.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS04318915
Source datasetuspto-grants-1982_03
ORD IDord-df4650ce70d3411b8f839c5bd6f8b53e
Source noteuspto-grants-1982_03