HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ammonia → HCID 178483214, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ammonia | HCID 222 | — |
| Reactant | Hydrazine hydrate (1:1) | HCID 24654 | — |
| Reactant | [3-[3-(1-piperidinylmethyl)phenoxy]propyl]-1H-1,2,4-triazole-3,5-diamine | HCID 21297553 | — |
| Reactant | HCID 178503920 | HCID 178503920 | — |
| Solvent | Water | HCID 962 | — |
| Solvent | Isopropanol | HCID 3776 | — |
| Solvent | Ethyl Acetate | HCID 8857 | — |
| Product | HCID 178483214 | HCID 178483214 | — |
Reaction Steps
Similarly prepared from N'-cyano-N-[3-[3-(1-piperidinylmethyl)phenoxy]propyl]-carbamimidothioic acid, methyl ester (14.1 g) and hydrazine hydrate (10 ml) was N3 -[3-[3-(1-piperidinylmethyl)phenoxy]propyl]-1H-1,2,4-triazole-3,5-diamine (10.4 g) m.p. 100°-101.5°. TLC silica; ethyl acetate:water:isopropanol:0.088 ammonia 25:8:15:2; Rf 0.4.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04318913 |
| Source dataset | uspto-grants-1982_03 |
| ORD ID | ord-5da490ec174a4253bc3a181250bb5cc7 |
| Source note | uspto-grants-1982_03 |